2-AMINO-4-METHYL-4,5,6,7-TETRAHYDRO-1-BENZOTHIOPHENE-3-CARBONITRILE synthesis
- Product Name:2-AMINO-4-METHYL-4,5,6,7-TETRAHYDRO-1-BENZOTHIOPHENE-3-CARBONITRILE
- CAS Number:60598-69-8
- Molecular formula:C10H12N2S
- Molecular Weight:192.28
13017-64-6
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60598-69-8
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Yield:60598-69-8 97%
Reaction Conditions:
with sulfur;tetraethylammonium hexafluorophosphate;acetonitrile at 20;Electrolysis;Inert atmosphere;Gewald reaction;
References:
Feroci, Marta;Chiarotto, Isabella;Rossi, Leucio;Inesi, Achille [Advanced Synthesis and Catalysis,2008,vol. 350,# 17,p. 2740 - 2746] Location in patent:supporting information; experimental part