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ChemicalBook CAS DataBase List 6-METHYLAMINO-7-METHYL-5-NITROQUINOLINE
83407-41-4

6-METHYLAMINO-7-METHYL-5-NITROQUINOLINE synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 110 mg / 0.17 h / Ambient temperature
2: 500 mg / KNO3, conc. H2SO4 / 0.5 h / Ambient temperature
3: 360 mg / conc. H2SO4 / 0.5 h / 70 °C
4: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 1 h

References:

Kasai, Hiroshi;Nishimura, Susumu [Bulletin of the Chemical Society of Japan,1982,vol. 55,# 7,p. 2233 - 2235]