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ChemicalBook CAS DataBase List 6-Fluoro-1H-indazol-3-ol
862274-39-3

6-Fluoro-1H-indazol-3-ol synthesis

1synthesis methods
-

Yield:862274-39-3 81%

Reaction Conditions:

Stage #1: 4-fluoroanthranilic acidwith hydrogenchloride;sodium nitrite in water at 10 - 20; for 11.5 h;Heating / reflux;
Stage #2: with sodium hydrogencarbonate in water; pH=5.5;

References:

WO2005/73199,2005,A1 Location in patent:Page/Page column 33-34

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