6'-ETHOXY-2'-HYDROXYACETOPHENONE 98 synthesis
2synthesis methods
- Product Name:6'-ETHOXY-2'-HYDROXYACETOPHENONE 98
- CAS Number:2750-25-6
- Molecular formula:C10H12O3
- Molecular Weight:180.2
Preparation by reaction of ethyl iodide on 2,6-dihydroxy acetophenone with potassium carbonate in refluxing acetone (64%).
Yield:2750-25-6 53%
Reaction Conditions:
with potassium carbonate in acetone at 55; for 8 h;
References:
Kondo, Hikaru;Akiba, Nana;Kochi, Takuya;Kakiuchi, Fumitoshi [Angewandte Chemie - International Edition,2015,vol. 54,# 32,p. 9293 - 9297][Angew. Chem.,2015,vol. 127,# 32,p. 9425 - 9429,5] Location in patent:supporting information