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ChemicalBook CAS DataBase List 6-CHLOROINDOLE-3-ACETONITRILE
61220-58-4

6-CHLOROINDOLE-3-ACETONITRILE synthesis

4synthesis methods
-

Yield:-

Reaction Conditions:

Stage #1: 6-chloroindolewith eschenmoser's salt;acetic acid in acetonitrile at 20; for 4 h;
Stage #2: methyl iodide in ethanol at 20; for 18 h;
Stage #3: sodium cyanide in water;N,N-dimethyl-formamide at 70; for 4 h;

References:

Egami, Hiromichi;Hotta, Ryo;Otsubo, Minami;Rouno, Taiki;Niwa, Tomoki;Yamashita, Kenji;Hamashima, Yoshitaka [Organic Letters,2020,vol. 22,# 14,p. 5656 - 5660] Location in patent:supporting information

773837-37-9 Synthesis
sodium:cyanide

773837-37-9
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