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ChemicalBook CAS DataBase List (6-BroMobenzo[b]thiophen-2-yl)Methanol
374933-76-3

(6-BroMobenzo[b]thiophen-2-yl)Methanol synthesis

8synthesis methods
105191-64-8 Synthesis
Ethyl 6-broMo-1-benzothiophene-2-carboxylate

105191-64-8
59 suppliers
$55.00/250mg

-

Yield:374933-76-3 96%

Reaction Conditions:

with lithium borohydride in tetrahydrofuran at 60; for 3 h;

Steps:

3 3. Preparation of (6-bromo-benzo[b]thiophen-2-yl)-methanol

(a) tetrahydrofuran, LiBH4, 60° C., 3 h [0308] The substance was obtained according to the general procedure, yielding the title compound as a white solid (96%)

References:

US2014/303207,2014,A1 Location in patent:Paragraph 0307; 0308