6-aMinobenzo[c][1,2]oxaborol-1(3H)-ol synthesis
- Product Name:6-aMinobenzo[c][1,2]oxaborol-1(3H)-ol
- CAS Number:117098-94-9
- Molecular formula:C7H8BNO2
- Molecular Weight:148.95
99-55-8
415 suppliers
$6.00/25g
117098-94-9
69 suppliers
$70.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: hydrogen bromide; sodium nitrite / water / 0.5 h / 0 °C
1.2: 1 h / 25 °C
2.1: N-Bromosuccinimide; dibenzoyl peroxide / acetonitrile / 24 h / 100 °C / Schlenk technique; Inert atmosphere
3.1: water; 1,4-dioxane / 1 h / 60 °C
3.2: 60 °C
4.1: zinc / 1 h / 20 °C
References:
Fuscaldo, Rodrigo S.;Vontobel, Pedro H. V.;Boeira, Eduam O.;Moro, Angélica V.;Costa, Jessie S. da [European Journal of Organic Chemistry,2019,vol. 2019,# 10,p. 2050 - 2055]
118803-40-0
80 suppliers
$27.00/250mg
117098-94-9
69 suppliers
$70.00/100mg
5735-41-1
174 suppliers
$8.00/250mg
117098-94-9
69 suppliers
$70.00/100mg
40138-16-7
344 suppliers
$9.00/1g
117098-94-9
69 suppliers
$70.00/100mg
957062-84-9
65 suppliers
$33.00/1g
117098-94-9
69 suppliers
$70.00/100mg