6-ACRYLOYL-2-DIMETHYLAMINONAPHTHALENE synthesis
- Product Name:6-ACRYLOYL-2-DIMETHYLAMINONAPHTHALENE
- CAS Number:86636-92-2
- Molecular formula:C15H15NO
- Molecular Weight:225.29
3900-45-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
2.1: calcium hydride / tetrahydrofuran / 0.08 h / Inert atmosphere
2.2: Reflux; Inert atmosphere
3.1: sodium hydroxide / toluene / 12 h / Reflux
References:
CN112645828, 2021, A
1000210-73-0
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5043-03-8
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305835-80-7
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15231-91-1
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