5-Methyl-4-hexenoic acid methyl ester synthesis
- Product Name:5-Methyl-4-hexenoic acid methyl ester
- CAS Number:35901-76-9
- Molecular formula:
- Molecular Weight:0
1445-45-0
353 suppliers
$10.00/5mL
115-18-4
187 suppliers
$10.00/5g
802294-64-0
1 suppliers
inquiry
35901-76-9
0 suppliers
inquiry
Yield:35901-76-9 98%
Reaction Conditions:
at 125; for 12 h;
Steps:
i Example i
Synthesis of compound I-1. In the flask, add trimethyl orthoacetate (1 mol), 2-methyl-3-buten-2-ol (1 mol) and propionic acid (0.2 mol), then heat the reaction system to 125°C, and continue to stir the reaction 12h, the reaction was stopped.Washed with water, saturated NaHCO3and saturated brine successively, dried over anhydrous sodium sulfate, and distilled under reduced pressure at 30 hPa and 70 °C to obtain compound I (yield 98%).
References:
CN114315497,2022,A Location in patent:Paragraph 0048-0051
71899-05-3
0 suppliers
inquiry
35901-76-9
0 suppliers
inquiry
43219-18-7
0 suppliers
inquiry
35901-76-9
0 suppliers
inquiry
32853-30-8
28 suppliers
$27.00/100mg
35901-76-9
0 suppliers
inquiry