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ChemicalBook CAS DataBase List 5-methyl-1,1'-biphenyl-2-amine
42308-28-1

5-methyl-1,1'-biphenyl-2-amine synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,4-dioxane; water / 12 h / 90 °C / Inert atmosphere
2: tin(II) chloride dihdyrate / ethanol / 5 h / 75 °C

References:

Yuan, Ming;Chen, Li;Wang, Junwei;Chen, Shenjie;Wang, Kongchao;Xue, Yongbo;Yao, Guangmin;Luo, Zengwei;Zhang, Yonghui [Organic Letters,2015,vol. 17,# 2,p. 346 - 349]