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ChemicalBook CAS DataBase List 5-Hydroxypyrimidine
26456-59-7

5-Hydroxypyrimidine synthesis

4synthesis methods
-

Yield:-

Reaction Conditions:

with hydrogen;palladium 10% on activated carbon in methanol at 20;

Steps:


D136 pyrimidin-5-ol To a solution of 5-[(phenylmethyl)oxy]pyrimidine (2.43 g, 13.0 mmol) in methanol (20 mL) was added Pd/C (10 % Pd/C, 10 % on carbon). The reaction mixture was stirred at room temperature under H2 atmosphere over weekend, then filtered and concentrated. The residue was used into next step without purification.

References:

GLAXO GROUP LIMITED;WAN, Zehong;ZHANG, Xiaomin;TONG, Zhaolong;LONG, Kai;DOWDELL, Sarah E.;MANAS, Eric Steven;GOODMAN, Krista Beaver WO2012/37782, 2012, A1 Location in patent:Page/Page column 58-59

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