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ChemicalBook CAS DataBase List 5,6-DIMETHOXY-2-METHYL-BENZOTHIAZOLE
62306-04-1

5,6-DIMETHOXY-2-METHYL-BENZOTHIAZOLE synthesis

6synthesis methods
107963-01-9 Synthesis
N-(3,4-DIMETHOXYPHENYL)THIOACETAMIDE

107963-01-9
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Yield:62306-04-1 17%

Reaction Conditions:

with iron(III) chloride;N-Bromosuccinimide;1-butyl-3-methylimidazolium trifluoromethanesulfonimide in acetonitrile at 40; for 2 h;Inert atmosphere;regioselective reaction;

References:

Henry, Martyn C.;Abbinante, Vincenzo Mirco;Sutherland, Andrew [European Journal of Organic Chemistry,2020,vol. 2020,# 19,p. 2819 - 2826]

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