5-(4-TRIFLUOROMETHYL-PHENYL)-CYCLOHEXANE-1,3-DIONE synthesis

2synthesis methods

Product Name:5-(4-TRIFLUOROMETHYL-PHENYL)-CYCLOHEXANE-1,3-DIONE
CAS Number:55579-69-6
Molecular formula:C13H11F3O2
Molecular Weight:256.22

455-19-6 Synthesis

455-19-6
415 suppliers
$6.00/5g

5-(4-TRIFLUOROMETHYL-PHENYL)-CYCLOHEXANE-1,3-DIONE

55579-69-6
31 suppliers
$111.16/Price $/250mgs:

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 32 percent / 50percent aq. NaOH / 72 h / Ambient temperature
2: EtONa / ethanol / 6 h / Heating
3: 2 N NaOH / 2 h / Heating
4: 5 N H₂SO₄ / 4.5 h / Heating

References:

Kesten, Stephen J.;Degnan, Margaret J.;Hung, Jocelyn;McNamara, Dennis J.;Ortwine, Daniel F.;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 19,p. 3429 - 3447]

1-[4-(TRIFLUOROMETHYL)PHENYL]BUT-1-EN-3-ONE

80992-93-4
45 suppliers
$24.00/250mg

55579-69-6
31 suppliers
$111.16/Price $/250mgs:

References

5-(4-TRIFLUOROMETHYL-PHENYL)-CYCLOHEXANE-1,3-DIONE Related Search:

5-PHENYLCYCLOHEXANE-1,3-DIONE 3-PHENYL-CYCLOHEXANONE 1,3-Cyclohexanedione 1-(1-ETHYL-PROPYL)-4-METHYL-BENZENE 1-CYCLOHEXYL-4-METHYL-BENZENE 5-(4-METHYLPHENYL)CYCLOHEXANE-1,3-DIONE 5-METHYLCYCLOHEXANE-1,3-DIONE