Methyl 2,3,4-tris-O-(phenylmethyl)-beta-D-glucopyranosiduronic acid synthesis
- Product Name:Methyl 2,3,4-tris-O-(phenylmethyl)-beta-D-glucopyranosiduronic acid
- CAS Number:4356-82-5
- Molecular formula:C28H30O7
- Molecular Weight:478.53
709-50-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 1,4-diaza-bicyclo[2.2.2]octane / dichloromethane
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C
3: iron(III) chloride hexahydrate; triethylsilane / dichloromethane
4: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 0 - 20 °C
References:
Wan, I. C. Steven;Witte, Martin D.;Minnaard, Adriaan J. [Organic Letters,2019,vol. 21,# 18,p. 7669 - 7673]