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ChemicalBook CAS DataBase List 4-tert-Butylaniline
769-92-6

4-tert-Butylaniline synthesis

6synthesis methods
-

Yield:769-92-6 97%

Reaction Conditions:

with hydrogen in ethanol at 25 - 30; for 6 h;

Steps:

General procedure for hydrogenation of nitro arylto amino aryl (1a)

General procedure: Nitro aryl compound (4.06 mmol) stirred in the presence of CPIP (50 mg) and under hydrogen atmosphere in ethanol (20 ml) for 6 h. Reaction monitor on TLC. Catalyst recovered by filtration and amino aryl isolated by distillation of ethanol, isolated yield 99% (Table 5).

References:

Chundawat, Narendra Singh;Pathan, Sultan;Singh, Girdhar Pal;Deuri, Arup Saha;Zarrintaj, Payam;Chauhan, Narendra Pal Singh [Chemical Papers,2021,vol. 75,# 6,p. 2835 - 2850]

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