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ChemicalBook CAS DataBase List 4-NITROPHTHALOXIME
105969-98-0

4-NITROPHTHALOXIME synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 65 percent / hydrogen chloride / 24 h / Heating
2: 68 percent / 1.) hydroxylamine, KOH, 2.) 12 percent HCl / ethanol; methanol / 1.) a) 0-4 deg C, 6 h, b) RT, 48 h

References:

Chan;Lien;Tokes [Journal of Medicinal Chemistry,1987,vol. 30,# 3,p. 509 - 514]

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