4-HYDROXY-7,8-DIMETHOXYQUINOLINE synthesis
- Product Name:4-HYDROXY-7,8-DIMETHOXYQUINOLINE
- CAS Number:99878-76-9
- Molecular formula:C11H11NO3
- Molecular Weight:205.21
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1) nBuLi, N,N,N',N'tetramethylethylenediamine; 2) trimethylsilylmethyl azide / 1) ether, hexane, 22 degC, 18.5 h.; 2) ether, hexane, 22 degC, 3.5 h.
2: 1) MeOH, 22 degC, 4 d.; 2) diphenyl ether, reflux, 25 min.
References:
Kelly, T. Ross;Maguire, Martin P. [Tetrahedron,1985,vol. 41,# 15,p. 3033 - 3036]
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