4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL synthesis
- Product Name:4-HYDRAZINO-BENZOIC ACID ETHYL ESTER HCL
- CAS Number:40566-85-6
- Molecular formula:C9H13ClN2O2
- Molecular Weight:216.67
5798-75-4
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Yield:40566-85-6 95%
Reaction Conditions:
Stage #1: Ethyl 4-bromobenzoatewith nickel(II) bromide trihydrate;(4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate;1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide at 120; for 0.166667 h;Irradiation;Flow reactor;
Stage #2: with hydrogenchloride in 1,4-dioxane at 20; for 4 h;Inert atmosphere;
References:
Mata, Alejandro;Tran, Duc N.;Weigl, Ulrich;Williams, Jason D.;Kappe, C. Oliver [Chemical Communications,2020,vol. 56,# 93,p. 14621 - 14624] Location in patent:supporting information
94-09-7
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![1,2,3-Oxadiazolium, 3-[4-(ethoxycarbonyl)phenyl]-5-hydroxy-, inner salt](/CAS/20211123/GIF/89101-11-1.gif)
89101-11-1
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40566-85-6
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