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ChemicalBook CAS DataBase List 4-(HEPTYLOXY)-4'-BIPHENYLCARBOXYLIC ACID
59748-17-3

4-(HEPTYLOXY)-4'-BIPHENYLCARBOXYLIC ACID synthesis

2synthesis methods
-

Yield:59748-17-3 91%

Reaction Conditions:

Stage #1: 4'-Hydroxybiphenyl-4-carboxylic acidwith potassium hydroxide in ethanol;water; for 1 h;Reflux;
Stage #2: 1-Bromoheptanewith potassium iodide in ethanol;water; for 36 h;Reflux;
Stage #3: with sulfuric acid in water;

References:

Marini;Domenici;Malanga;Menicagli;Veracini [Tetrahedron,2010,vol. 66,# 19,p. 3472 - 3477] Location in patent:experimental part

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