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ChemicalBook CAS DataBase List 4-fluoro-7-hydroxy-1-indanone
136191-16-7

4-fluoro-7-hydroxy-1-indanone synthesis

3synthesis methods
The raw material compound was mixed with aluminum chloride and then the reaction was heated to 100 °C. After 15 minutes, heat the reactants to 180 °C. Cool the mixture to room temperature after 3 h. Add ethyl acetate to the reaction solution and stir for 2 h. The resulting organic phase is dried on anhydrous sodium sulfate and concentrated under reduced pressure. After purification, 4-fluoro-7-hydroxy-1-indanone was obtained.
4-FLUORO-7-HYDROXY-1-INDANONE
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: triethylamine
2: AlCl3

References:

Aktiebolaget Astra US5376687, 1994, A

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