4-(ETHYLTHIO)BENZENEBORONIC ACID synthesis
- Product Name:4-(ETHYLTHIO)BENZENEBORONIC ACID
- CAS Number:145349-76-4
- Molecular formula:C8H11BO2S
- Molecular Weight:182.05
106-53-6
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$12.00/1g
145349-76-4
143 suppliers
$10.00/1g
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 94 percent / NaOH / tetrahydrofuran; H2O / 1 h / 100 °C
2.1: n-BuLi / tetrahydrofuran / 2 h / -78 °C
2.2: B(OMe)3 / tetrahydrofuran / -78 - 20 °C
2.3: 66 percent / 20percent HCl
References:
Percec;Bera;De Binod;Sanai;Smith;Holerca;Barboiu;Grubbs;Frechet [Journal of Organic Chemistry,2001,vol. 66,# 6,p. 2104 - 2117]
30506-30-0
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$26.60/5g
145349-76-4
143 suppliers
$10.00/1g