4'-CARBOETHOXY-2,2-DIMETHYLPROPIOPHENONE synthesis
- Product Name:4'-CARBOETHOXY-2,2-DIMETHYLPROPIOPHENONE
- CAS Number:62985-52-8
- Molecular formula:C14H18O3
- Molecular Weight:234.29
51934-41-9
296 suppliers
$6.00/5g
3282-30-2
371 suppliers
$19.85/100ml
62985-52-8
11 suppliers
$417.00/1g
Yield:62985-52-8 83%
Reaction Conditions:
Stage #1: 4-iodobenzoic acid ethyl esterwith lithium dineopentylcuprate in tetrahydrofuran at -30; for 2 h;
Stage #2: pivaloyl chloride in tetrahydrofuran at 20;
References:
Piazza, Claudia;Knochel, Paul [Angewandte Chemie - International Edition,2002,vol. 41,# 17,p. 3263 - 3265]
51934-41-9
296 suppliers
$6.00/5g
630-19-3
328 suppliers
$13.00/1g
62985-52-8
11 suppliers
$417.00/1g
5798-75-4
198 suppliers
$6.00/5g
3282-30-2
371 suppliers
$19.85/100ml
62985-52-8
11 suppliers
$417.00/1g
3282-30-2
371 suppliers
$19.85/100ml
62985-52-8
11 suppliers
$417.00/1g
3282-30-2
371 suppliers
$19.85/100ml
131379-16-3
24 suppliers
$285.00/50mL
62985-52-8
11 suppliers
$417.00/1g