4-BROMO-4'CARBOETHOXYBENZOPHENONE synthesis
- Product Name:4-BROMO-4'CARBOETHOXYBENZOPHENONE
- CAS Number:746651-80-9
- Molecular formula:C16H13BrO3
- Molecular Weight:333.18
1344727-27-0
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Yield:746651-80-9 62%
Reaction Conditions:
Stage #1: (4-(ethoxycarbonyl)phenyl)zinc pivalatewith chloro-trimethyl-silane;copper(I) cyanide di(lithium chloride) in tetrahydrofuran at 0; for 0.5 h;Inert atmosphere;
Stage #2: 4-chlorobenzoyl chloride in tetrahydrofuran at 25; for 4 h;Inert atmosphere;
References:
Manolikakes, Sophia M.;Ellwart, Mario;Stathakis, Christos I.;Knochel, Paul [Chemistry - A European Journal,2014,vol. 20,# 38,p. 12289 - 12297] Location in patent:supporting information
51934-41-9
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746651-80-9
9 suppliers
$294.00/1g