4-Bromo-2-propyl thiophene synthesis
- Product Name:4-Bromo-2-propyl thiophene
- CAS Number:36155-79-0
- Molecular formula:C7H9BrS
- Molecular Weight:205.12
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Yield:36155-79-0 90%
Reaction Conditions:
Stage #1: 1-(4-bromo-thien-2-yl)-1-propanonewith hydrazine hydrate monohydrate in ethylene glycol dimethyl ether at 160; for 0.75 h;Wolff-Kishner Reduction;
Stage #2: with potassium hydroxide in ethylene glycol dimethyl ether at 35 - 160; for 1.5 h;
References:
Bar, Sukanta;Martin, Maxwell I. [Canadian Journal of Chemistry,2022,vol. 100,# 8,p. 601 - 605]
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$10.00/5g
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