4,6,6-Trimethyl(6H)-1,3-thiazin-2-amine synthesis
2synthesis methods
- Product Name:4,6,6-Trimethyl(6H)-1,3-thiazin-2-amine
- CAS Number:2953-81-3
- Molecular formula:C7H12N2S
- Molecular Weight:156.25
Yield:2953-81-3 95%
Reaction Conditions:
Stage #1: 4-methyl-pent-3-en-2-one;thioureawith hydrogenchloride in ethanol at 20; for 1 h;
Stage #2: with triethylamine in dichloromethane at 20; for 4 h;
References:
Landreau, Cyrille;Deniaud, David;Reliquet, Alain;Meslin, Jean Claude [Synthesis,2002,# 3,p. 403 - 408]
