4-(4-METHOXYPHENOXY)BENZOIC ACID 97 synthesis
- Product Name:4-(4-METHOXYPHENOXY)BENZOIC ACID 97
- CAS Number:3525-22-2
- Molecular formula:C14H12O4
- Molecular Weight:244.24
50793-28-7
1 suppliers
inquiry
3525-22-2
33 suppliers
$46.00/1g
Yield:3525-22-2 94%
Reaction Conditions:
with water;sodium hydroxide in ethanol at 70; for 3 h;
Steps:
1.D-3.2 The synthesis of DI-7
PI - 6 (0.09 g, 0.33 mmol) was added NaOH (0.13 g, 3.30 mmol) in EtOH/H20 (10: 1) solution. The mixture was heated to reflux for 3 h. The mixture was cooled to room temperature and evaporated. The mixture was dissolved in water and slowly acidified with 10% aq. HC1 and extracted with CH2CI2. The extract was dried over MgS04, filtered, and concentrated to afford PI - 7 (0.08 g, 94%) as white solid.
References:
WO2015/158908,2015,A1 Location in patent:Page/Page column 91
38342-84-6
12 suppliers
inquiry
3525-22-2
33 suppliers
$46.00/1g
26002-36-8
9 suppliers
inquiry
3525-22-2
33 suppliers
$46.00/1g
