5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide synthesis
- Product Name:5-Chloro-6'-Methyl-3-[4-(Methylsulfonyl)phenyl]-2,3'-bipyridine 1'-Oxide
- CAS Number:325855-74-1
- Molecular formula:C18H15ClN2O3S
- Molecular Weight:374.84
221615-75-4
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325855-74-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: t-BuOK / tetrahydrofuran / 0.75 h / 20 °C
1.2: 85 percent / AcOH; TFA; NH2OH*HCl / tetrahydrofuran; H2O / 5 h / Heating
2.1: 89 percent / mCPBA
References:
Davies, Ian W.;Marcoux, Jean-Francois;Reider, Paul J. [Organic Letters,2001,vol. 3,# 2,p. 209 - 211]
202409-33-4
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325855-74-1
65 suppliers
$125.00/50mg