3-Tert-butyl-5-methylsalicylicacid synthesis
- Product Name:3-Tert-butyl-5-methylsalicylicacid
- CAS Number:23050-96-6
- Molecular formula:C12H16O3
- Molecular Weight:208.25
2409-55-4
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23050-96-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 84 percent / p-toluenesulfonic acid, 4A molecular sieves / CH2Cl2 / 72 h / Heating
2: 1.) TMEDA, n-BuLi / 1.) Et2O, from -50 deg C to -5 deg C, 4 h, 2.) Et2O, RT, overnight
3: glacial acetic acid / 1 h / Heating
References:
Katritzky;Lang;Lan [Synthetic Communications,1993,vol. 23,# 8,p. 1175 - 1182]
71313-39-8
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23050-96-6
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![1H-Isoindol-1-one, 3-[3-(1,1-dimethylethyl)-2-hydroxy-5-methylbenzoyl]-2,3-dihydro-2-(4-methylphenyl)-](/CAS/20210305/GIF/95646-21-2.gif)
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23050-96-6
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