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ChemicalBook CAS DataBase List 3-Phenylpyruvic acid
156-06-9

3-Phenylpyruvic acid synthesis

9synthesis methods
-

Yield:156-06-9 15%

Reaction Conditions:

with water;ruthenium trichloride; pH=4.5 at 100; for 24 h;Product distribution / selectivity;

Steps:

27
[Example 27]; 0.1 mmol of water-soluble acetylene dicarboxylic acids whose R1 is C6H5 and R2 is H in Fig. 1(a) was mixed with 2 mL of aqueous solution containing 1.0 μmol of ruthenium trichloride, and the mixture was reacted at the pH 4.5 at 100°C under argon atmosphere for 24 hours. The resulting reaction mixture was condensed to give a product. The product was analyzed by 1H NMR.

References:

Japan Science and Technology Agency EP1932824, 2008, A1 Location in patent:Page/Page column 20; 21

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