3-Hydroxypropionitrile synthesis
- Product Name:3-Hydroxypropionitrile
- CAS Number:109-78-4
- Molecular formula:C3H5NO
- Molecular Weight:71.08
Yield:109-78-4 97.3%
Reaction Conditions:
with aluminum oxide;boron trifluoride diethyl etherate in propylene glycol at -10 - 10; for 28 h;Reagent/catalyst;Temperature;
Steps:
7 Example 7
2.70 g of hydrogen cyanide and 4.40 g of ethylene oxide were charged into a closed reactor equipped with a cooling device,Stir; then add 1.0g white solid in Example 5, the reaction was stirred at -10 4h,The reaction was stirred at 10 ° C for another 24h. After the reaction is completed, a small amount of sodium hypochlorite is not involved in the reaction of cyanideHydrogen after the detection of 3-hydroxy-propionitrile content. The results show that under this condition,The yield of 3-hydroxypropionitrile was as high as 97.3%.
References:
Jiangnan University;Zhang Lei;Teng Qiliang;Wu Lei;Hu Xueyi;Fang Yun CN106883142, 2017, A Location in patent:Paragraph 0030; 0031; 0032; 0033; 0034; 0035; 0036-0048
107-13-1
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$16.00/25ML
109-78-4
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$10.00/1g
107-13-1
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108-95-2
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$14.00/25g
3055-86-5
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$47.00/1g
109-78-4
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$10.00/1g
107-13-1
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$16.00/25ML
1656-48-0
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109-78-4
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$10.00/1g
