3'-FLUOROBIPHENYL-2-CARBALDEHYDE synthesis
- Product Name:3'-FLUOROBIPHENYL-2-CARBALDEHYDE
- CAS Number:676348-32-6
- Molecular formula:C13H9FO
- Molecular Weight:200.21
17318-03-5
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$60.00/100mg
![2-Propanamine, N-[(2-methoxyphenyl)methylene]-2-methyl-](/CAS/20210305/GIF/82632-38-0.gif)
82632-38-0
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676348-32-6
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Yield:676348-32-6 95%
Reaction Conditions:
Stage #1: N-tert-butyl-1-(2-methoxyphenyl)methaniminewith chromium dichloride in tetrahydrofuran at 25; for 0.0833333 h;Schlenk technique;Inert atmosphere;
Stage #2: bromo(3-fluorophenyl)magnesium in tetrahydrofuran at 25; for 5 h;Schlenk technique;Inert atmosphere;
Stage #3: with hydrogenchloride in tetrahydrofuran;water at 25; for 3 h;Schlenk technique;Inert atmosphere;
References:
Cong, Xuefeng;Tang, Huarong;Zeng, Xiaoming [Journal of the American Chemical Society,2015,vol. 137,# 45,p. 14367 - 14372] Location in patent:supporting information
768-35-4
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6630-33-7
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676348-32-6
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7022-45-9
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$22.00/250mg
676348-32-6
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135-02-4
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676348-32-6
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579-72-6
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$45.00/100mg
676348-32-6
25 suppliers
$290.00/1g