3-ethyl-1-phenyl-2-thioxoimidazolidin-4-one synthesis
- Product Name:3-ethyl-1-phenyl-2-thioxoimidazolidin-4-one
- CAS Number:37021-14-0
- Molecular formula:C11H12N2OS
- Molecular Weight:220.29
2216-92-4
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$47.00/5G
542-85-8
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$52.00/25mL
37021-14-0
8 suppliers
$495.43/5MG
Yield:37021-14-0 54%
Steps:
VI 1-phenyl-3-ethyl-2-thiohydantoin STR12
EXAMPLE VI 1-phenyl-3-ethyl-2-thiohydantoin STR12 A mixture of ethyl-N-phenyl glycinate (17.9 grams, 0.1 mole) and ethylisothiocyanate (13.1 grams, 0.15 moles) was refluxed for 5 hours and allowed to stand overnight at room temperature (21° C.). The resulting solid was ground up and crystallized from ethanol to produce 12 grams (54% yield) of the above-identified product having a melting point of about 122° C.
References:
US4473393,1984,A