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ChemicalBook CAS DataBase List 3-Chlorophenylisopropyl ketone
55649-98-4

3-Chlorophenylisopropyl ketone synthesis

7synthesis methods
-

Yield:55649-98-4 450 mg

Reaction Conditions:

Stage #1: C10H13ClOwith oxalyl dichloride in dichloromethane;dimethyl sulfoxide at -78; for 1 h;Inert atmosphere;
Stage #2: with triethylamine in dichloromethane;dimethyl sulfoxide at 20;

References:

Lackner, Aaron D.;Samant, Andrew V.;Toste, F. Dean [Journal of the American Chemical Society,2013,vol. 135,# 38,p. 14090 - 14093] Location in patent:supporting information