3-Amino-5-chloropicoline synthesis
- Product Name:3-Amino-5-chloropicoline
- CAS Number:89639-36-1
- Molecular formula:C6H7ClN2
- Molecular Weight:142.59
21427-62-3
233 suppliers
$6.00/1g
89639-36-1
60 suppliers
$65.00/100mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 3.83 h / 20 °C / Inert atmosphere
1.2: 12.5 h / Reflux
1.3: pH 9
2.1: tin(II) chloride dihdyrate / ethyl acetate / 3 h / 85 °C / Inert atmosphere
References:
GLAXOSMITHKLINE LLC;BOBKO, Mark, A.;DARCY, Michael, G.;EVANS, Karen, A.;FAITG, Thomas, H.;KAURA, Arun, Chandar;PENG, Xin;SARPONG, Martha, A.;SEEFELD, Mark, A.;SU, Dai-shi WO2012/149102, 2012, A1
1211533-93-5
87 suppliers
$10.00/100mg
89639-36-1
60 suppliers
$65.00/100mg
78607-32-6
206 suppliers
$5.00/250mg
13061-96-6
301 suppliers
$6.00/1g
89639-36-1
60 suppliers
$65.00/100mg