ChemicalBook CAS DataBase List 3-AMINO-3-(4-NITROPHENYL)PROPIONIC ACID

3-AMINO-3-(4-NITROPHENYL)PROPIONIC ACID synthesis

6synthesis methods

Product Name:3-AMINO-3-(4-NITROPHENYL)PROPIONIC ACID
CAS Number:35005-61-9
Molecular formula:C9H10N2O4
Molecular Weight:210.19

100-01-6
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79-10-7 Synthesis

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35005-61-9
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Yield:-

Reaction Conditions:

in water at 20;Heating;

Steps:

2.1. Preparation

The starting compounds, 4-nitroaniline (Aldrich, 99%) and acrylic acid (Aldrich, 94%) was used as supplied and prepared in the ratio of 1:1. The dissolved acid was added to the hot solution of 4-nitroaniline. Next the solution was cooled to room temperature and it remained clear. The solution slowly evaporated during a few days till the crystals appeared.

References:

Marchewka;Drozd;Janczak [Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy,2011,vol. 79,# 4,p. 758 - 766] Location in patent:experimental part