3,5-DIIODO-4-HYDROXYBENZHYDRAZIDE synthesis
- Product Name:3,5-DIIODO-4-HYDROXYBENZHYDRAZIDE
- CAS Number:89011-17-6
- Molecular formula:C7H6I2N2O2
- Molecular Weight:403.94
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 66 percent / 1) KI, 2) HIO3 / 1) aq. EtOH, 2N acetic acid, reflux, 2) water, reflux, 2 h
2: aq. HCl; tetrahydrofuran / 3 h / Heating
References:
Heindel;Van Dort;Cahn;et al. [Journal of Heterocyclic Chemistry,1985,vol. 22,# 1,p. 209 - 210]
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