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ChemicalBook CAS DataBase List 3,5-DIFLUORO-2-NITROANILINE
361-72-8

3,5-DIFLUORO-2-NITROANILINE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: water / 1.5 h / 0 - 20 °C
2: sulfuric acid; nitric acid / dichloromethane / 18 h / 0 - 20 °C
3: hydrogenchloride / water / 4 h / 100 °C

References:

Jovené, Cyril;Jacquet, Morgane;Marrot, Jérome;Bourdreux, Flavien;Kletsky, Mikhail E.;Burov, Oleg N.;Gon?alves, Anne-Marie;Goumont, Régis [European Journal of Organic Chemistry,2014,vol. 2014,# 29,p. 6451 - 6466]