3,4,5-Trimethoxybenzyl alcohol synthesis
- Product Name:3,4,5-Trimethoxybenzyl alcohol
- CAS Number:3840-31-1
- Molecular formula:C10H14O4
- Molecular Weight:198.22
86-81-7
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$16.26/10gm:
3840-31-1
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$28.00/25g
Yield:3840-31-1 100%
Reaction Conditions:
with sodium tetrahydroborate in methanol at 0 - 20; for 4 h;
Steps:
Typical Procedures for the Preparation of Compounds 6A'- G' and 7A'- H'.
General procedure: To a solution of 3,4-dimethoxybenzaldehyde (1 g, 6 mmol) in methanol was added NaBH4 (0.27, 7.2 mmol) at 0 °C. The reaction mixture was stirred at room temperature for 4 h, quenched with 3% aqueous HCl solution, and evaporated to dryness. The residue was extracted with CH2Cl2 and the organic layer was dried with MgSO4. Evaporation of the dried organic layer yielded 0.96g (3,4-dimethoxyphenyl)methanol (6D0) as a white solid.
References:
Kim, Sung-Soo;Fang, Yuanying;Park, Haeil [Bulletin of the Korean Chemical Society,2015,vol. 36,# 6,p. 1676 - 1680] Location in patent:supporting information
1916-07-0
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3840-31-1
210 suppliers
$28.00/25g
86-81-7
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$16.26/10gm:
6443-69-2
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$6.00/5g
3840-31-1
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$28.00/25g
118-41-2
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$14.00/5g
3840-31-1
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$28.00/25g
67-56-1
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86-81-7
472 suppliers
$16.26/10gm:
6443-69-2
285 suppliers
$6.00/5g
3840-31-1
210 suppliers
$28.00/25g
75921-68-5
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