3,3-DIMETHYLPIPERIDINE synthesis
- Product Name:3,3-DIMETHYLPIPERIDINE
- CAS Number:1193-12-0
- Molecular formula:C7H15N
- Molecular Weight:113.2
681-57-2
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1193-12-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: thionyl chloride / 5 h / Heating
2.1: 1,2-dimethoxy-ethane / 15 h / Heating
2.2: 8 h / 200 °C
3.1: 80 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating
4.1: 54 percent / hydrogen / Pd/C / methanol / 20 °C
References:
Berardi, Francesco;Ferorelli, Savina;Colabufo, Nicola Antonio;Leopoldo, Marcello;Perrone, Roberto;Tortorella, Vincenzo [Bioorganic and Medicinal Chemistry,2001,vol. 9,# 5,p. 1325 - 1335]
125943-36-4
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1193-12-0
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6140-61-0
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1193-12-0
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1194-33-8
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1193-12-0
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133003-98-2
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1193-12-0
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