3-(2-HYDROXYETHYL)PYRIDINE synthesis
- Product Name:3-(2-HYDROXYETHYL)PYRIDINE
- CAS Number:6293-56-7
- Molecular formula:C7H9NO
- Molecular Weight:123.15
6419-36-9
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Yield: 95.5%
Steps:
P.28.1 (28-1)
(28-1) 2-(3-Pyridyl)ethanol 3-Pyridylacetic acid hydrochloride (25 g) was treated successively as in the above Production Examples 3-3 and 3-4 to give the title compound (16.938 g) as a yellow oil (yield: 95.5%). 1H-NMR (400 MHz, CDCl3): δ(ppm) 2.86(2H, t, J=6.8Hz), 3.88(2H, t, J=6.8Hz), 7.22(1H, dd, J=4.8, 7.6Hz), 7.527(1H, d, J=7.6Hz), 8.42(1H, dd, J=2.0, 4.8Hz), 8.44(1H, d, J=2.0Hz).
References:
39998-25-9
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7424-56-8
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39931-77-6
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6293-56-7
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1000210-73-0
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6293-56-7
120 suppliers
$20.00/100mg