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ChemicalBook CAS DataBase List 3-(1,1-dioxothiomorpholin-4-yl)phenylamine
1152859-34-1

3-(1,1-dioxothiomorpholin-4-yl)phenylamine synthesis

2synthesis methods
585-79-5 Synthesis
3-Bromonitrobenzene

585-79-5
3 suppliers
$15.00/1g

3-(1,1-dioxothiomorpholin-4-yl)phenylamine

1152859-34-1
8 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium carbonate / 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane / Reflux
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 10 - 15 °C
3: hydrogen / palladium 10% on activated carbon / methanol / Inert atmosphere

References:

WO2012/59932,2012,A1

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