(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID synthesis

4synthesis methods

Product Name:(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID
CAS Number:214193-13-2
Molecular formula:C6H9NO2
Molecular Weight:127.14

1,2-Pyrrolidinedicarboxylic acid, 5-hydroxy-, 1-(1,1-diMethylethyl) 2-ethyl ester, (2S)-

194594-23-5
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(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID

214193-13-2
29 suppliers
$65.00/2.5mg

Yield:-

Steps:

Multi-step reaction with 5 steps
1: PPTS
2: NH₄Cl / 150 °C / 20 - 100 Torr
3: 65 percent / Et₂Zn / 1,2-dichloro-ethane; hexane / a) 0 deg C, 30 min, b) RT, 6 h
4: DMAP, Et₃N / CH₂Cl₂
5: 1.) aq. LiOH, 2.) HCO₂H / 1.) MeOH

References:

Hanessian, Stephen;Reinhold, Ulrich;Saulnier, Michel;Claridge, Stephen [Bioorganic and Medicinal Chemistry Letters,1998,vol. 8,# 16,p. 2123 - 2128]

1,2-Pyrrolidinedicarboxylic acid, 5-Methoxy-, 1-(1,1-diMethylethyl) 2-ethyl ester, (2S)-

194594-24-6
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214193-13-2
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References

178172-26-4 Synthesis

(S)-1-Boc-2,3-dihydro-2-pyrrolecarboxylic acid ethyl ester

178172-26-4
108 suppliers
$144.00/250mg

214193-13-2
29 suppliers
$65.00/2.5mg

References

2-Azabicyclo[3.1.0]hexane-2,3-dicarboxylic acid, 2-(1,1-dimethylethyl) 3-ethyl ester, (1S,3S,5S)-

214193-11-0
30 suppliers
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214193-13-2
29 suppliers
$65.00/2.5mg

References

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(1S,3S,5S)-2-AZABICYCLO[3.1.0]HEXANE-3-CARBOXYLIC ACID synthesis