2-Octanone oxime synthesis
- Product Name:2-Octanone oxime
- CAS Number:7207-49-0
- Molecular formula:C8H17NO
- Molecular Weight:143.2267
111-13-7
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Yield:7207-49-0 87%
Reaction Conditions:
with hydroxylamine hydrochloride in pyridine at 20; for 120 h;
Steps:
3 EXAMPLE 3; Synthesis of 2-Octanone Oxime
In a 50 ml round-bottom flask, a mixture of 2-octanone, hydroxylamine hydrochloride in pyridine was stirred, at room temperature under nitrogen blanket, for five days. The reaction mixture was then concentrated under vacuum to remove most of pyridine. The oil was then dissolved in dichloromethane. The product precipitated on standing. The product was obtained as a white solid in 87% yield.
References:
US6696608,2004,B1 Location in patent:Page column 20
18023-52-4
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