2-(Methylthio)-5-nitrobenzonitrile synthesis
- Product Name:2-(Methylthio)-5-nitrobenzonitrile
- CAS Number:74631-35-9
- Molecular formula:C8H6N2O2S
- Molecular Weight:194.21
6361-21-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: S,NH3 / methanol / 6 h / 80 °C
2: 1) NaOMe / 1) methyl glycol, 4 h, 80 deg C, 2) 1 h, 80 deg C
References:
Markert, Juergen;Hagen, Helmut [Liebigs Annalen der Chemie,1980,# 5,p. 768 - 778]
