2-METHYLBICYCLO[2.2.1]-5-HEPTENE-2-CARBOXYLIC ACID synthesis
- Product Name:2-METHYLBICYCLO[2.2.1]-5-HEPTENE-2-CARBOXYLIC ACID
- CAS Number:825-03-6
- Molecular formula:C9H12O2
- Molecular Weight:152.19
![Bicyclo[2.2.1]hept-5-ene-2-carboxaldehyde, 2-methyl-](/CAS/20210305/GIF/40441-67-6.gif)
40441-67-6
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825-03-6
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$60.00/100mg
Yield:825-03-6 99%
Reaction Conditions:
Stage #1: 5-formyl-5-methylbicyclo[2.2.1]hept-2-enewith sodium hydroxide;silver(l) oxide in water at 90; for 12 h;
Stage #2: with hydrogenchloride in water at 20; pH=2;
References:
Hatano, Manabu;Mizuno, Tomokazu;Izumiseki, Atsuto;Usami, Ryota;Asai, Takafumi;Akakura, Matsujiro;Ishihara, Kazuaki [Angewandte Chemie - International Edition,2011,vol. 50,# 51,p. 12189 - 12192] Location in patent:supporting information; experimental part
