ChemicalBook CAS DataBase List 2-METHYL-4-CYANOPHENYLBORONIC ACID

2-METHYL-4-CYANOPHENYLBORONIC ACID synthesis

1synthesis methods

Product Name:2-METHYL-4-CYANOPHENYLBORONIC ACID
CAS Number:313546-18-8
Molecular formula:C8H8BNO2
Molecular Weight:160.97

41963-20-6
183 suppliers
$15.00/1g

313546-18-8
103 suppliers
$27.00/250mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 0.25 h / -98 °C
1.2: tetrahydrofuran; hexane / 3.5 h / -98 - 20 °C
2.1: 0.63 g / aq. HCl / diethyl ether

References:

Stones, Duane;Manku, Sukhdev;Lu, Xiaosong;Hall, Dennis G. [Chemistry - A European Journal,2004,vol. 10,# 1,p. 92 - 100]

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2-METHYL-4-CYANOPHENYLBORONIC ACID synthesis

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