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ChemicalBook CAS DataBase List 2-Methyl-3-nitrophenol
5460-31-1

2-Methyl-3-nitrophenol synthesis

7synthesis methods
2-Methyl-3-nitrophenol was used as internal standard to develop a method for measurement of stable isotope ratio of methylnitrophenols in atmospheric particulate matter. It can be synthesized by the nitration of 2-Methoxy-3-MethylbenzenaMine.
-

Yield:-

Steps:

Multi-step reaction with 4 steps
2: nitric acid
3: concentrated hydrochloric acid
4: beim Diazotieren und Verkochen der schwefelsauren Diazoniumloesung

References:

Simonsen;Nayak [Journal of the Chemical Society,1915,vol. 107,p. 833]

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