2-iodo-4'-Methyl-1,1'-biphenyl synthesis
- Product Name:2-iodo-4'-Methyl-1,1'-biphenyl
- CAS Number:14385-93-4
- Molecular formula:C13H11I
- Molecular Weight:294.13
1204-43-9
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Yield:14385-93-4 90%
Reaction Conditions:
Stage #1: 4'-methylbiphenyl-2-aminewith hydrogenchloride;NaNO2 in lithium hydroxide monohydrate at 0 - 5; for 1 h;
Stage #2: with potassium iodide in lithium hydroxide monohydrate at 20;
References:
Chen, Dushen;Shi, Guangfa;Jiang, Hang;Zhang, Yu;Zhang, Yanghui [Organic Letters,2016,vol. 18,# 9,p. 2130 - 2133] Location in patent:supporting information
615-42-9
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5720-05-8
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615-43-0
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