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ChemicalBook CAS DataBase List (2-fluoro-4-methoxyphenyl)hydrazine hydrochloride
940298-93-1

(2-fluoro-4-methoxyphenyl)hydrazine hydrochloride synthesis

1synthesis methods
-

Yield:940298-93-1 56%

Reaction Conditions:

Stage #1: 2-fluoro-4-(methoxy)anilinewith hydrogenchloride;sodium nitrite in water at 0; for 1.5 h;
Stage #2: with hydrogenchloride;tin(ll) chloride at 0; for 4 h;Further stages.;

References:

Heredia-Moya, Jorge;Hayakawa, Yoshio;Kirk, Kenneth L. [Journal of Fluorine Chemistry,2006,vol. 127,# 9,p. 1256 - 1260]

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