2-Chloropropane synthesis
- Product Name:2-Chloropropane
- CAS Number:75-29-6
- Molecular formula:C3H7Cl
- Molecular Weight:78.54
187737-37-7
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78-87-5
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$14.00/25g
75-29-6
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$20.00/25mL
67-63-0
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$17.00/25ML
67-64-1
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$19.10/10ml
Yield:67-63-0 1087 μmol ，75-29-6 80.1 μmol ，67-64-1 18.8 μmol ，78-87-5 15.6 μmol
Reaction Conditions:
with copper(l) chloride;sodium chloride;copper dichloride at 150; for 0.25 h;Reagent/catalyst;Temperature;
Steps:
1; 2; 6; 7 Experiment 2:
A solution of CuCl2(0.71 mol/kg), CuCl (0.71 mol/kg), and NaCl (2.76 mol/kg) was heated in a Parr reactor under propylene pressure to 150°C for 15 minutes. The reactor was depressurized into a bubbler trap at 0°C to capture volatile compounds. When the reactor was opened, the solution was extracted three times with an organic solvent, e.g. ethyl acetate or dichloromethane, which was analyzed with a gas chromatograph equipped with a mass spectrometer. A total of 15.6 umol DCP and 62.4 umol PCH were measured. The amounts of recyclable products measured were 1087 umol isopropanol, 18.8 umol acetone, and 80.1 umol isopropyl chloride.
References:
WO2018/222642,2018,A1 Location in patent:Paragraph 161-163; 168; 169
187737-37-7
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75-29-6
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$20.00/25mL
67-63-0
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$17.00/25ML
75-29-6
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74-93-1
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1912-24-9
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75-29-6
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834-12-8
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75-29-6
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$20.00/25mL